Lead hydroxyapatites (PbHAp) have been prepared from H3PO4 and Pb(NO3)2 β’ 5PbO (1), the latter of which was obtained through dehydration of basic lead nitrates such as 2Pb(NO3)2 β’ 5Pb(OH)2 (2) and Pb(NO3)2 β’ 5Pb(OH)2 (3). The amount of 2 with respect to 3, as well as the quantity of an unidentified
Preparation and Characterization of Carbonated Barium Hydroxyapatites
β Scribed by Akemi Yasukawa; Manami Nakajima; Kazuhiko Kandori; Tatsuo Ishikawa
- Publisher
- Elsevier Science
- Year
- 1999
- Tongue
- English
- Weight
- 251 KB
- Volume
- 212
- Category
- Article
- ISSN
- 0021-9797
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β¦ Synopsis
Carbonated barium hydroxyapatite (Ba10(PO4)6(OH)2-2x(CO3)x, X = 0.30-0.57, BaHAP) particles with different Ba/P molar ratios were prepared by a wet method. CO2-3 ions were incorporated into OH- sites of a BaHAP lattice during the preparation at high solution pH. The obtained BaHAP particles were well crystallized and showed a high thermostability. On elevating the mixing temperature of H3PO4 and Ba(OH)2 solutions, the mean particle size of BaHAP particles decreased and their specific surface area increased. The amount of CO2 adsorbed irreversibly on BaHAP particles increased with an increase of their Ba/P molar ratio. Copyright 1999 Academic Press.
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