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Preparation and characterization of a poly(methyloctadecylsiloxane) thermally immobilized onto zirconized silica stationary phase for high-performance liquid chromatography

✍ Scribed by Carla G.A. da Silva; Carol H. Collins


Book ID
113536365
Publisher
Elsevier Science
Year
2012
Tongue
English
Weight
787 KB
Volume
1232
Category
Article
ISSN
1873-3778

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Chromatographic silica (10 lm) was chemically modified with the silylating agent: [3-(2-aminoethyl)aminopropyl]trimethoxysilane (AEAPTS). The reaction product was characterized by elemental analysis and infrared and 13 C and 29 Si NMR spectra. The chemically modified silica was treated with Cu(II) i