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Preparation and characterization of (24R and 24S)-5μ-cholestane-3α, 7α,24,25-tetrols and (24R and 24S)-5β-cholestane-3α, 24, 25-triols

✍ Scribed by A.K. Batta; B. Dayal; G.S. Tint; S. Shefer; V. Toome; G. Salen; E.H. Mosbach


Book ID
118978462
Publisher
Elsevier Science
Year
1978
Tongue
English
Weight
657 KB
Volume
31
Category
Article
ISSN
0039-128X

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Bile alcohol glucuronides: regioselectiv
✍ Bishambar Dayal; Gerald Salen; Janak Padia; Sarah Shefer; George S. Tint; Gino S 📂 Article 📅 1993 🏛 Elsevier Science 🌐 English ⚖ 746 KB

## ABSTRAm A facile and regiocontrolled procedure for the preparation of S~-cholestane-3a,7c,l2~,25-tetrol-3-O-fi-o-glucuronide and its corresponding C-26 analogue is described. The method involves direct coupling of bile alcohols, namely, 5/3-cholestane-3rY,7~,12a,25-tetrol and 24-nor-Sp-cholesta