Practical NMR spectroscopy laboratory guide : using Bruker spectrometers

✍ Scribed by Harwood, John S.; Mo, Huaping

• Publisher: Academic Press
• Year: 2016
• Tongue: English
• Leaves: 128
• Edition: 1
• Category: Library

✦ Synopsis

Practical NMR Spectroscopy Laboratory Guide is designed to provide non-expert NMR users, typically graduate students in chemistry, an introduction to various facets of practical solution-state NMR spectroscopy. Each chapter offers a series of hands-on exercises, introducing various NMR concepts and experiments and guiding the reader in running these experiments using an NMR spectrometer. The book is written for use with a Bruker NMR spectrometer running TopSpin software versions 1 or 2. This practical resource functions both as a text for instructors of a practical NMR course and also as a reference for spectrometer administrators or NMR facility directors when doing user training. This guide serves as serve as excellent, practical resource on its own or as a companion book to Timothy Claridge’s High-Resolution NMR Techniques in Organic Chemistry, 2nd Edition (Elsevier, 2009).

• Written by experts in solution-state NMR spectroscopy
• Provides step-by-step instructions for more than 50 activities using a Bruker NMR spectrometer
• Includes detailed appendices and sample questions for lab reports

✦ Table of Contents

Content:
Front-matter,Copyright,Acknowledgments,IntroductionEntitled to full textChapter 1 - Basics and Spectrometer Performance Checks, Pages 1-23
Chapter 2 - Multiple Irradiation and Multiple Pulse Experiments, Pages 25-38
Chapter 3 - Polarization Transfer and Its Applications, Pages 39-50
Chapter 4 - Homonuclear Correlation Experiments, Pages 51-60
Chapter 5 - PFG (Pulsed Field Gradient) Experiments, Pages 61-73
Chapter 6 - Introduction to NMR of Biomolecules in H2O, Pages 75-97
Chapter 7 - Selective Experiments Using Shaped Pulses, Pages 99-112
Chapter 8 - Diffusion Measurements and DOSY (Diffusion Ordered SpectroscopY), Pages 113-121