Powder study of hydrochlorothiazide form II
✍ Scribed by Florence, Alastair ;Johnston, Andrea ;Fernandes, Philippe ;Shankland, Kenneth ;Stevens, Howard N. E. ;Osmundsen, Sigrunn ;Mullen, Alexander B.
- Publisher
- International Union of Crystallography
- Year
- 2005
- Tongue
- English
- Weight
- 258 KB
- Volume
- 61
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Final observed (points), calculated (line) and difference [(y obs À y calc )/ (y obs )] profiles for the Rietveld refinement of the title compound.
📜 SIMILAR VOLUMES
The crystal structure of a new polymorph of the title compound, C 8 H 12 N + ÁC 10 H 11 O 2 À , was solved by simulated annealing from laboratory X-ray powder diffraction data, collected at 295 K. Subsequent Rietveld refinement using data collected to 1.54 A ˚resolution yielded an R wp of 0.029. The
A polycrystalline sample of a new polymorph of the title compound, C~8~H~11~NO~2~, was produced during a variable-temperature X-ray powder diffraction study. The crystal structure was solved at 1.67 Å resolution by simulated annealing from laboratory powder data collected at 250 K. Subsequent Rietve
The title compound, __cis__-[PtCl~2~(CH~3~NH~2~)~2~], was obtained from the reaction of K~2~PtCl~4~ with CH~3~NH~2~·HCl and CH~3~COOK. The single-crystal structure has been reported previously [Wimmer, Wimmer, Jaud, Johnson & Castan (1988). __Inorg. Chim. Acta__, 144, 25–30], but no three-dimensiona