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Potentiometric microdetermination of nitro- and bromophenols by oxidation with lodate and periodate

✍ Scribed by M.A. Zayed; H. Khalifa; F.A. Nour El-Dien

Publisher
Elsevier Science
Year
1987
Tongue
English
Weight
521 KB
Volume
35
Category
Article
ISSN
0026-265X

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The oxidation of 1-hexene and cyclohexene by molecular oxygen catalyzed by the iridium complexes [Ir(CH 3 CN) 4 NO 2 ](A) 2 (A=PF 6 (1) or BF 4 (2)) has been studied in acetonitrile under P(O 2 )=20 atm, T=120 β€’ C, substrate/catalyst=100, t=20 h. Both complexes are active for oxidizing 1-hexene to 1