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Polynuclear Complexes of Macrocyclic Oxamide with Thiocyanate: Syntheses, Crystal Structures and Magnetic Properties

✍ Scribed by Ya-Qiu Sun; Dong-Zhao Gao; Wen Dong; Dai-Zheng Liao; Chen-Xi Zhang

Publisher
John Wiley and Sons
Year
2009
Tongue
English
Weight
38 KB
Volume
2009
Category
Article
ISSN
1434-1948

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Three new polynuclear Mn II complexes with chloroacetate bridges were obtained and characterized by X-ray diffraction: 2), and [Mn(Β΅-ClCH 2 COO) 2 (phen)] n (3). The Mnβ€’β€’β€’Mn distance for 1 (3.624 A ˚) is smaller than for 2 (4.613 A ˚) and 3 (4.530 A ˚); this is in agreement with the number of carbox