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Polymorphism of an Organolithium Compound: Dilithium 1,2-diphenylbenzocyclobutadienediide · 2 Tetramethylethylenediamine

✍ Scribed by Prof. Dr. Gernot Boche; Dr. Heinz Etzrodt; Priv.-Doz. Dr. Werner Massa; Gerhard Baum

Publisher
John Wiley and Sons
Year
1985
Tongue
English
Weight
245 KB
Volume
24
Category
Article
ISSN
0044-8249

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< 5 % of its cis isomer (NMR spectrum) as a yellow oil which gradually solidified. The hexafluorophosphate (yield 86 %) forms colorless crystals (from acetone/ether) which decompose between 79 and 80°C.