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Polymorphism in the Crystal Structure of the Cellulose Fragment Analogue Methyl 4-O-Methyl-β-D-Glucopyranosyl-(1-4)-β-D-Glucopyranoside

✍ Scribed by Anna Rencurosi; Jürgen Röhrling; Jutta Pauli; Antje Potthast; Christian Jäger; Serge Pérez; Paul Kosma; Anne Imberty

Publisher: John Wiley and Sons
Year: 2002
Tongue: English
Weight: 158 KB
Volume: 114
Category: Article
ISSN: 0044-8249
DOI: 10.1002/1521-3757(20021115)114:22<4453::aid-ange4453>3.0.co;2-d

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Structure of 4-(N′-Pivaloyl)-D(L)-Phenyl

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subjected to-an X-ray diffraction analysis. C20H29N303S.CH OH.H20, Mr=441.58, triclinic, Pol, a = 12.98;;2), b = 9.939(1), c = 11.345(1)w, a = 75.05(1)', .31 cm-', F(000) = 476, T = 291K, R = 0.058 for 3875 observed reflections. The data reveal a molecular conformation with all t r a n s amide bond