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Polyhaloheterocyclic compounds. Part XXXI—carbon-13 NMR spectra as a structural probe for polychloroaromatic compounds

✍ Scribed by Richard D. Chambers; Raymond S. Matthews; W. Kenneth; R. Musgrave; Peter G. Urben


Publisher
John Wiley and Sons
Year
1980
Tongue
English
Weight
347 KB
Volume
13
Category
Article
ISSN
0749-1581

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✦ Synopsis


Abstract

Carbon‐13 spectra of twelve chlorofluoropyridines (C~5~CI~n~F~5−n~N), of known structure, have been assigned and an assessment has been made of the degree of additivity of substituent chemical shifts (SCS). Reasonable additivity is observed for pyridine derivatives but little regulatiry can be inferred from the spectra of perchlorinated‐diazines and ‐triazines. There is an approximately linear relationship between ^13^C and ^19^F chemical shifts.