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Platinum-Catalyzed Aromatic C—H Silylation of Arenes with 1,1,1,3,5,5,5-Heptamethyltrisiloxane.

✍ Scribed by Miki Murata; Naoaki Fukuyama; Jun-ichi Wada; Shinji Watanabe; Yuzuru Masuda

Publisher: John Wiley and Sons
Year: 2007
Weight: 24 KB
Volume: 38
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.200750184

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## Abstract Fused tricyclic 7‐phenyl‐5__H__‐thizolo[5,4‐__e__]pyrrolo[1,2‐__a__][1,4]diazepin‐10(9__H__)one (**10**) was prepared by thermolysis of 2‐phenyl‐4‐(1‐pyrrolylmethyl)thiazole‐5‐carbonyl azide (**9**) in acetic acid. In addition, starting from **10**, 7‐phenyl‐5__H__‐thiazolo [5,4‐__e__][