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Plasma and blood assay of xanthine and hypoxanthine by gas chromatography-mass spectrometry: physiological variations in humans

โœ Scribed by C. Lartigue-Mattei; J.L. Chabard; H. Bargnoux; J. Petit; J.A. Berger; J.M. Ristori; J.L. Bussiere; P. Catilina; M.J. Catilina

Book ID
108449657
Publisher
Elsevier Science
Year
1990
Weight
577 KB
Volume
529
Category
Article
ISSN
0378-4347

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We present an assay for 2,3-butanediol by gas chromatography-mass spectrometry of its trimethylsilyl ethers. 2R,3R- and/or 2S,3S-2,3-butanediol and meso-2,3-butanediol are quantitated with corresponding internal standards of [2,3-2H2]butanediol. Limits of detection are 1 and 0.1 microM for split and