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Planar β-Linked Oligothiophenes Based on Thieno[3,2- b ]thiophene and Dithieno[3,2- b :2‘,3‘- d ]thiophene Fused Units

✍ Scribed by San Miguel, Lidaris; Porter, William W.; Matzger, Adam J.


Book ID
121442530
Publisher
American Chemical Society
Year
2007
Tongue
English
Weight
105 KB
Volume
9
Category
Article
ISSN
1523-7060

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A convenient and improved synthesis of d
✍ Fredrik Allared; Jonas Hellberg; Tommi Remonen 📂 Article 📅 2002 🏛 Elsevier Science 🌐 French ⚖ 52 KB

An improved synthesis of dithieno[3,2-b:2%,3%-d]thiophene 1 is presented. By starting from 2,3-dibromothiophene 2 the total yield was improved from 35 to 58%. We also describe a more convenient synthesis of one of the reagents, benzenesulfonic acid thioanhydride 3.