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Photolysis of methyl 2-chloro-3-oxobutanoate

✍ Scribed by V. Enev; I. Petkov; L. Markova; P. Markov

Publisher
Elsevier Science
Year
1987
Weight
660 KB
Volume
39
Category
Article
ISSN
0047-2670

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Odorless and Practical Thioacetalization Reagent: Methyl 2-(1,3-Dithian-2-ylidene)-3-oxobutanoate
✍ Sun Ran; Liu Qun; Yu Hai-Feng; Zhao Yu-Long; Liu Jun; Ouyang Yan; Dong De-Wen πŸ“‚ Article πŸ“… 2005 πŸ› John Wiley and Sons 🌐 English βš– 62 KB

## Abstract α‐Oxo ketene dithioacetals, methyl 2‐(1,3‐dithian/dithiolan‐2‐ylidene)‐3‐oxobutanoate (**2a/2b**) prepared in nearly quantitative yields simply from methyl acetylacetate, carbon disulfide and 1,3‐dibromopropane/1,2‐dibro‐ moethane in the presence of potassium carbonate, were investigate