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Photoinduced template synthesis of cyclobutane-containing crown ether

✍ Scribed by I. G. Ovchinnikov; O. V. Fedorova; P. A. Slepukhin; G. L. Rusinov

Book ID
106520770
Publisher
Springer
Year
2008
Tongue
English
Weight
212 KB
Volume
57
Category
Article
ISSN
1573-9171

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A series of benzo-crown ethers containing the thiazole subcyclic moity have been synthesized. Reaction of 1,2-bis(thioamidomethyloxy)benzene 2 with ethyl bromopyruvate in ethanol provided 1,2-bis(thiazolyl)benzene \(4(80 \%)\) along with thiazole \(5(14 \%)\). Reduction of 4 with lithium aluminum hy