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Photocyclisation of Diphenylamine as a Fluorogenic Reaction for Photochemical-Fluorimetric Analysis

✍ Scribed by C. A. T. Fall; A. Diop; J. J. Aaron

Book ID
101761148
Publisher
Wiley (John Wiley & Sons)
Year
2010
Weight
432 KB
Volume
95
Category
Article
ISSN
0037-9646

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Upon irradiation, 5-dicyanomethylenebicyclo[2.2.2]octene (2) gives a highly strained compound, 2,2-dicyanotricyclo[4.2.1.01'3]nonene (6) in good yield. Of additional interest is the observation that the starting material 3 can be quantitatively regenerated from the photoproduct 6 with release of 28.