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Photochemistry of 8,8,9,9-tetramethyl-1,3,4,6,7,8-hexahydro-1,4-ethanonaphthalene-2,5-dione, a δ-oxo-β,γ-unsaturated ketone

✍ Scribed by Ralf Kilger; Wolfgang Körner; Paul Margaretha

Publisher
John Wiley and Sons
Year
1984
Tongue
German
Weight
159 KB
Volume
67
Category
Article
ISSN
0018-019X

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## Abstract The 6‐(3‐hydroxypropylamino)‐3‐methylpyrimidine‐2,4‐dione (1) did not afford the expected 6‐(3‐chloro‐propylamino)‐ derivative on reaction with thionyl chloride, but, instead, the pyrimidine rings were joined __via__ a sulfur bridge to give 9,9′‐thiobis(1,2,3,4,7,8‐hexahydro‐7‐melnyl‐6_