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Photochemistry of 2-Alkoxymethyl-5-methylphenacyl Chloride and Benzoate

✍ Scribed by Plíštil, Lukáš; Šolomek, Tomáš; Wirz, Jakob; Heger, Dominik; Klán, Petr

Book ID
126822514
Publisher
American Chemical Society
Year
2006
Tongue
English
Weight
281 KB
Volume
71
Category
Article
ISSN
0022-3263

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## Abstract Methyl 3‐azido‐5‐__O‐tert__‐butyldiphenylsilyl‐2,3‐dideoxy‐D‐__erythro__‐furanoside (3) was coupled with silylated 5‐hydroxymethyluracil (1a) and its C~1~‐C~6~ alkyl ethers 1b–g to give the corresponding protected nucleosides 4a‐g which were deprotected with Bu~4~NF to afford 3‐azido nu