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Photochemistry of 1-carbomethoxy-6-methyltricyclo[4.3.1.04,6]Dec-2-en-10-one. preparation of a 1,3-cyclooctadiene

โœ Scribed by Arthur G Schultz; Kan K Eng; Rudolph K Kullnig

Publisher
Elsevier Science
Year
1986
Tongue
French
Weight
217 KB
Volume
27
Category
Article
ISSN
0040-4039

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Base-catalysed rearrangement of a 2-alkynyl-tetrahydropyran generates an allenol ether intermediate which undergoes acid-catalysed cyclisation to the 1,6-dioxaspiro[4S]dec-3-ene system. We recently described a synthesis of the 1,7-dioxaspiro[5S]undec-4-ene system (4)' which made strategic use of th