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Photochemical Generation and Matrix-Isolation Detection of Dimethylvinylidene

✍ Scribed by Reed, Sasha C.; Capitosti, Gregory J.; Zhu, Zhendong; Modarelli, David A.

Book ID
120544938
Publisher
American Chemical Society
Year
2001
Tongue
English
Weight
228 KB
Volume
66
Category
Article
ISSN
0022-3263

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## Abstract Irradiation of squaric acid (4) in an argon matrix at 10 K leads to ethynediol (dihydroxyacetylene) (1) via bis (hydroxyketenyl) 5 and deltic acid (6). The identification of 1 is based on the comparison between the experimental and calculated IR spectrum.