Photochemical chlorination of chloro(3,3,3-trifluoropropyl) silanes and the synthesis of chloro(3,3,3-trifluoropropenyl)silanes
β Scribed by M. A. Kadina; V. A. Ponomarenko
- Book ID
- 112420331
- Publisher
- Springer
- Year
- 1965
- Tongue
- English
- Weight
- 334 KB
- Volume
- 14
- Category
- Article
- ISSN
- 1573-9171
No coin nor oath required. For personal study only.
π SIMILAR VOLUMES
## Abstract Infrared spectra of 3,3,3βtrifluoropropylsilane (CF~3~CH~2~CH~2~SiH~3~) and 3,3,3βtrifluoropropylsilaneβ__d__~3~ (CF~3~ CH~2~CH~2~SiD~3~) were obtained in the vapour, liquid, and crystalline solid phases in the range 4000β50 cm^β1^. Additional spectra in argon matrices at 5 K were recor
It has been demonstrated that 7,7-dichlorobicyclo[4.l.O]hept-3-enes are excellent precursors to benzocyclopropenes. l-4 We report here an application of this method to the synthesis of the functionalized benzocyclopropenes 1 and 2, potential precursors to cyclopropabenzynes 3 and 4.