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Photo[2+2]Cycloaddition Reaction of Maleic Acid Anhydride

✍ Scribed by M. M. Abou-Elzahab; M. A. Metwally; A. M. Dawidar; M. Abdel-Mogib

Publisher
John Wiley and Sons
Year
1989
Tongue
English
Weight
168 KB
Volume
331
Category
Article
ISSN
1615-4150

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2. A mixture of KH[PH03] and 40% H F (molar ratio 1 : 1.5) is evaporated to dryness over P4O10 and KOH in a vacuum desiccator. After a few days, the crystalline mass (or sometimes syrup) is extracted with methanol as above. Method 1 is superior to the other. Elemental analysis (K, P, F) confirmed t