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Phosphorus(V) Isocyanates

✍ Scribed by L. I. Samaraj; O. I. Kolodjažnij; Prof. Dr. G. I. Derkatsch

Publisher
John Wiley and Sons
Year
1968
Tongue
English
Weight
116 KB
Volume
7
Category
Article
ISSN
0044-8249

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📜 SIMILAR VOLUMES

Phosphor(v)-isocyanate
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A mixture of 12.5 g of 2,2-dimethyl-l,3-dioxolan and 25 ml of glacial acetic acid is added to 10 grams of addition product (3). The mixture is then stirred and heated to 60°C. The diazonium salt dissolves, and after 10 minutes, the reaction is completed. After working up as described above, 89.3 % o