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Phosphorus-31 chemical shift anisotropy in solid nucleic acids

✍ Scribed by Terao, Takehiko; Matsui, Shigeru; Akasaka, Kazuyuki


Book ID
125942089
Publisher
American Chemical Society
Year
1977
Tongue
English
Weight
417 KB
Volume
99
Category
Article
ISSN
0002-7863

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The principal componenls or the 3'P chemical shirt baser in six phosphonic acid suers and ~\\TJ phosphonic acids xverr determined. The chemical shirl anisorropies of the es~crs lie in rhr range herween 149 and 182 ppm and the asymmcq paramekrs between 0.1 and 0.5.

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## Abstract An approach to spinning sideband (SSB) separation of protonated and non‐protonated carbons in slow spinning conditions via dipolar dephasing is proposed. This method offers two features: SSB spectral simplification, which greatly reduces the overlaps encountered in a usual SSB spectrum,