𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Phosphomolybdic Acid (PMA)–SiO2 as a Heterogeneous Solid Acid Catalyst for the One-Pot Synthesis of 2H-Indazolo[1,2-b]phthalazine-triones

✍ Scribed by Gowravaram Sabitha; Chitti Srinivas; Avula Raghavendar; Jhillu Singh Yadav


Publisher
John Wiley and Sons
Year
2010
Tongue
German
Weight
149 KB
Volume
93
Category
Article
ISSN
0018-019X

No coin nor oath required. For personal study only.

✦ Synopsis


Abstract

Phosphomolybdic acid (PMA)–SiO~2~ was found to be an efficient catalyst for the three‐component condensation reaction of phthalhydrazide, 1,3‐diketone, and aldehydes to produce 2__H__‐indazolo[1,2‐b]phthalazine‐triones in excellent yields. The catalyst can be recovered and reused without significant loss of activity.


📜 SIMILAR VOLUMES


Synthesis and application of silica phen
✍ Hojat Veisi; Alireza Sedrpoushan; Mohammad Ali Zolfigol; Farajollah Mohanazadeh 📂 Article 📅 2011 🏛 Journal of Heterocyclic Chemistry 🌐 English ⚖ 302 KB

## Abstract Silica phenyl sulfonic acid (SPSA) was prepared and effectively used in the one‐pot synthesis of 2‐aryl‐1‐arylmethyl‐1H‐1,3‐benzimidazoles from __o__‐phenylenediamine with aldehydes in water in the presence of tetrabutyl ammonium bromide with good to high yield. Also, SPSA was used as a

Oxalic acid as a versatile catalyst for
✍ Jaiprakash N. Sangshetti; Devanand B. Shinde; Nagnnath D. Kokare 📂 Article 📅 2008 🏛 Journal of Heterocyclic Chemistry 🌐 English ⚖ 242 KB 👁 1 views

## Abstract magnified image 3,4‐Dihydropyrimidin‐2‐(1__H__)‐ones and their thione analogues are synthesized from the condensation of aromatic aldehydes, β‐dicarbonyl compound and urea or thiourea in presence of 5 mol% of oxalic acid in ethanol‐water (1:2; v/v) under mild reaction conditions. The y