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Phenyl Ring Orientations in Two Tetracyclone Adducts; X-Ray Crystal Structures of exo -and endo -1,7,8,9-Tetraphenyltricyclo-[5.2.1.0 2,6 ]deca-3,8-dien-10-ones

✍ Scribed by Coxon, JM; O'Connell, MJ; Steel, PJ

Book ID
121330453
Publisher
Commonwealth Scientific and Industrial Research Organisation Publishing
Year
1985
Tongue
English
Weight
393 KB
Volume
38
Category
Article
ISSN
0004-9425

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1H-1,3-Diazepines, 5H-1,3-diazepines, 1,
1H-1,3-Diazepines, 5H-1,3-diazepines, 1,3-diazepinones, and 2,4-diazabicyclo[3.2.0]heptenesPreliminary reports on parts of this work have been published in ref 1. This paper is Diazepines, Part 3. For Part 2, see ref 2.,Electronic supplementary information (ESI) available: NMR spectra of 4a, 4c, 19v ? 20, 19a ? 25a, and 19g ? 25g (Fig. S1?S6), Arrhenius and Eyring plots for H-exchange in 4b,c (Fig. S7), views of the X-ray crystal structures of compounds 26 and 22bB (Fig. S8?S9), bond lengths and angles for compounds 4k, 22bB and 26, preparative procedures and characterization data for all compounds not described in the Experimental section, and computational data (Cartesian coordinates, absolute energies, IR, 1H and 13C NMR) for 20a?c, 21a?b, 22aA?F and 22aB dimer. See http://www.rsc.org/suppdata/ob/b3/b317099c/
✍ Reisinger, Ales; Koch, Rainer; Bernhardt, Paul V.; Wentrup, Curt πŸ“‚ Article πŸ“… 2004 πŸ› Royal Society of Chemistry 🌐 English βš– 496 KB