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Phenanthridinium cyclobisintercalands. Fluorescence sensing of AMP and selective binding to single-stranded nucleic acids

✍ Scribed by Ivo Piantanida; Barbara Susanne Palm; Predrag Cudic; Mladen Zinic; Hans-Jörg Schneider


Publisher
Elsevier Science
Year
2001
Tongue
French
Weight
89 KB
Volume
42
Category
Article
ISSN
0040-4039

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✦ Synopsis


Macrocyclic ligands 1 and 2 containing two positively charged phenanthridinium units and aminobisacetylenic bridges, exhibit significantly higher affinity toward single-stranded rather than double-stranded polynucleotides. The ligands bis-intercalate into the former and show non-intercalative interactions with the latter type of nucleic acids. Both ligands differentiate AMP from the GMP or UMP by significant fluorescence emission increase upon complexation of the first nucleotide in water (log K s of 1:1 and 1:2 complexes 5.8 and 1.4, respectively), while only a slight emission change is observed in titrations with GMP and UMP.