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Phase transition in [Ca(NH3)6](ClO4)2 studied by neutron scattering methods and far infrared spectroscopy

✍ Scribed by Joanna Hetmańczyk; Łukasz Hetmańczyk; Anna Migdał-Mikuli; Edward Mikuli; Ireneusz Natkaniec

Book ID: 116608442
Publisher: Elsevier Science
Year: 2011
Tongue: English
Weight: 408 KB
Volume: 509
Category: Article
ISSN: 0925-8388
DOI: 10.1016/j.jallcom.2011.03.125

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Four phase transitions at: T h C1 ¼ 267:1 K, T h C2 ¼ 258:8 K, T h C3 ¼ 254:1 K and T h C4 ¼ 195:4 K (on heating) and at T c C1 ¼ 263:8 K, T c C2 ¼ 255:4 K, T c C3 ¼ 246:0 K (on cooling) were determined for [Ca(H 2 O) 4 ](ClO 4 ) 2 between 90 and 295 K by means of differential scanning calorimetry