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Phase shifts induced by transient Bloch-Siegert effects in NMR

✍ Scribed by Lyndon Emsley; Geoffrey Bodenhausen

Book ID
107734860
Publisher
Elsevier Science
Year
1990
Tongue
English
Weight
528 KB
Volume
168
Category
Article
ISSN
0009-2614

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## Abstract Chemical shifts of silicon‐29 in 39 trimethylsiloxy derivatives of 5α‐ and 5β‐androstanes reported here satisfy an empirical linear correlation with terms describing molecular geometry. The steric ^29^Si chemical shifts are controlled by association of the silyl ethers with the hydrogen