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Periodate-permanganate oxidations. IV. Determination of the position of double bonds in unsaturated fatty acids and esters

โœ Scribed by E. von Rudloff

Book ID
112802461
Publisher
Springer-Verlag
Year
1956
Tongue
English
Weight
419 KB
Volume
33
Category
Article
ISSN
0003-021X

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The methyl esters of some mono-unsaturated fatty acids have been methylthiolated by the iodine-catalysed addition of dimethyl disulfide across the double bond. The resulting derivatives are suitable for gas chromatography. The fragmentation of the derivatives on electron impact yields mass spectra w