✦ LIBER ✦
Peak suppression in Fourier transform n.m.r.: Application of the selective excitation technique to the problem of 13C satellites in 31P resonance
✍ Scribed by R. K. Harris; R. H. Newman; A. Okruszek
- Publisher
- John Wiley and Sons
- Year
- 1977
- Tongue
- English
- Weight
- 258 KB
- Volume
- 9
- Category
- Article
- ISSN
- 0749-1581
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✦ Synopsis
Abstract
Selective pulsed excitation was used in a technique to suppress the resonance due to a per‐^12^C‐isotopomer so as to overcome dynamic range problems when observing ‘^13^C satellite’ lines. The technique was used to obtain nuclear spin parameters from the ^13^C satellites in ^31^P resonance for the racemic isomer of P,P′‐dimethyl‐P,P′‐diphenyldiphosphine disulphide, [MePhP(:S)]~2~.