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Palladium-dihalide complexes with carbonyl donors

✍ Scribed by Dolores Fregona; Zijian Guo; Giuseppina Faraglia; Sergio Sitran

Publisher
Springer
Year
1992
Tongue
English
Weight
516 KB
Volume
17
Category
Article
ISSN
0340-4285

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## Rhodium(I) carbonyl complexes, namely [Rh(CO)2C1L ] where L = thiourea (Tu), 1,3-diphenyl-2-thiourea (DTu), dithizone (Dtz), indole (Id), 3-chloropyridine (Clpy), 3hydroxypyridine (HOpy), 3-methylpyridine (Mepy), 2,5dimethylpyridine (Me2py) or 2,5-dichloropyridine (C12py)] were prepared. [Rh(CO

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General procedure: To a mixture of dry THF (10 mL) and the appropriate N ligand (5 mL) was added solid [(h 2 ,h 2 -nbd)(h 2 -ma)Pd 0 ] (0.15 g, 0.5 mmol). In the case of ammonia, 3-4 mL was condensed at Γ€70 8C, to which cold THF (10 mL) was slowly added, followed by the Pd 0 complex as above. After