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Palladium-catalyzed coupling reactions of 1-(tributylstannyl)-1-octen-3-ol

โœ Scribed by Stille, John K.; Sweet, Mark P.

Book ID
125931446
Publisher
American Chemical Society
Year
1990
Tongue
English
Weight
433 KB
Volume
9
Category
Article
ISSN
0276-7333

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Coupling reactions of 1-tributylstannyl-
Coupling reactions of 1-tributylstannyl-1-octen-3-ol catalyzed by palladium: The synthesis of PGB1 and coriolic acid
โœ J.K. Stille; Mark P. Sweet ๐Ÿ“‚ Article ๐Ÿ“… 1989 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 285 KB

The palladium catalyzed coupling of (S)-E-1 -tributylstannyl-1 -octen-3-01 (3) with 2-(6 carbethoxyhexyl)-3-iodo-2-cyclopenten-I-one gave a 70% yield of the (S)-ethyl ester of PGBI. Coriolic acid was synthesized in 75% yield by coupling 3 with Z-lo-iododecenoic acid, demonstrating the tolerance of t