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Palladium-catalyzed carbonylation of tert-butyl alcohol to esters of iso-valeric acid

✍ Scribed by Hongying Zhou; Shijie Lu; Hongqi Li; Jing Chen; Hongxiang Fu; Hanqing Wang

Publisher
Elsevier Science
Year
1997
Tongue
English
Weight
174 KB
Volume
116
Category
Article
ISSN
1381-1169

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Direct oxidation of primary alcohols to the corresponding carboxylic acids is performed highly efficiently at room temperature with anhydrous tert-butyl hydroperoxide in the presence of a catalytic amount of easily available CuCl under ligand free conditions in acetonitrile. Benzylic alcohols are mo