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P-Type gradient-enhanced COSY experiments show lower t1 noise than N-type

✍ Scribed by Timothy J. Horne; Gareth A. Morris


Publisher
John Wiley and Sons
Year
1997
Tongue
English
Weight
257 KB
Volume
35
Category
Article
ISSN
0749-1581

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✦ Synopsis


Many of the perturbations that lead to noise in 2D NMR spectroscopy cause Ñuctuations in the relative phases t 1 of pulses and coherences. Because the sensitivity of the phase of a coherence to changes in the phase of a pulse depends on the change of coherence order, P-type signals in homonuclear correlation experiments are insensitive to errors in the phase of the mixing pulse, and hence they show less noise than N-type signals. This e †ect is t 1 illustrated for the gradient COSY experiment.