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Ozonolysis of 2-(1,4-cyclohexadienyl)glycine

✍ Scribed by Gury Zvilichovsky; Vadim Gurvich


Publisher
Elsevier Science
Year
1995
Tongue
French
Weight
524 KB
Volume
51
Category
Article
ISSN
0040-4020

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distillation under high vacuum at room temperature (time required ca. 48 h). Double recrystallization of the residue from pentane afforded (2) in 50 to 55% yield (based on ( I ) ) . For conversion of (2) into (3) a solution of (2) (2.3 mmol) and Fe(CO), (3 ml) in ether (50 ml) was irradiated at -40