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Oxyfluorinated open framework compounds. XVIII Dehydration of single crystals of the iron phosphate ULM-12 or [Fe4(PO4)4F3(H2O)3,N2C6H14] with an open structure, structural determination and magnetic study of the dehydrated phase(ULM-19)

✍ Scribed by M. Cavellec; J.M. Grenèche; G. Férey

Publisher
Elsevier Science
Year
1998
Tongue
English
Weight
660 KB
Volume
20
Category
Article
ISSN
1387-1811

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✍ S. Mahesh; Mark A. Green; Srinivasan Natarajan 📂 Article 📅 2002 🏛 Elsevier Science 🌐 English ⚖ 485 KB

The hydrothermal syntheses and structures of two new open-framework iron phosphates, I, [C 6 N 2 H 14 ][Fe III 2 F 2 (HPO 4 ) 2 (H 2 PO 4 ) 2 ].2H 2 O, II, and [C 6 N 2 H 14 ] 2 [Fe III 3 (OH)F 3 (PO 4 ) (HPO 4 ) 2 ] 2 . H 2 O, are presented. The structures of both I and II consist of FeO 4 F 2 octa