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Oxidative cyclization ofN-alkyl-2-arylhydrazonothioacetamides

✍ Scribed by N. P. Belskaya; A. I. Bolgova; M. L. Kondrat’eva; O. S. El’tsov; V. A. Bakulev

Publisher: Springer
Year: 2011
Tongue: English
Weight: 324 KB
Volume: 60
Category: Article
ISSN: 1573-9171
DOI: 10.1007/s11172-011-0140-9

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CuC1,-Induced oxidative coupling of 2-(rertbutyl)-6,6-dimethylpentafulvenyl anion 9 predominantly takes place at C(7) and C(5) to give [7-71 and (7-51 coupling products 15 and 16 in 35 and 47% yields, respectively (Scheme 3 ) whose structures are elucidated from IDand 2D-NMR analysis. Compared with