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Oxidative Coupling in a Series of Derivatives of 4a,9-Diaza-1,2,4a,9a-tetrahydrofluorene. 6. Reactions with Substituted 2-Aminoethanols

✍ Scribed by O. Yu. Slabko; N. V. Ageenko; D. V Kuklev; V. A. Kaminski

Book ID: 110339987
Publisher: Springer US
Year: 2002
Tongue: English
Weight: 144 KB
Volume: 38
Category: Article
ISSN: 0009-3122
DOI: 10.1023/a:1015651707589

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Oxidative coupling of 4a,9-diaza-l,2,4a,9a-tetrahydro-gH-fluorene with primary amines and ammonia in the presence of MnO 2 gives the corresponding 6-aryl (or alkyl)imino-4a,9-diaza-l,2,4a,9a-tetrahydro-6H-fluorenes. Coupling with thiourea under these conditions affords 6-cyanoimino-4a,9-diaza-l,2,4

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