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Oxidative cleavage of ethers by metallic nitrates supported on silica gel

✍ Scribed by Nishiguchi, Takeshi; Bougauchi, Masahiro

Book ID: 125501690
Publisher: American Chemical Society
Year: 1990
Tongue: English
Weight: 500 KB
Volume: 55
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo00308a018

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Many metal nitrates, especially zinc(I1) and copper(I1) nitrates, supported on silica gel, oxidized secondary and benzylic alcohols to the corresponding ketones and aldehydes efficiently. The supported reagent technique has received increasing attention in recent years.l As one oxidizng reagent of a

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Thioacetals are cleaved into aldehydes and ketones, under very mild conditions, by K-10 clay-supported ferric or cupric nitrate. WIDESPREAD use is made of thioacetals in organic synthesis, mostly for protection or umpolung of the reactivity of a carbonyl groupI. Regeneration of the carbonyl function

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