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Oxidations by thionyl chloride. II. 3-Thietanones from ketones

โœ Scribed by Krubsack, Arnold J.; Higa, Tatsuo.; Slack, William E.


Book ID
127212860
Publisher
American Chemical Society
Year
1970
Tongue
English
Weight
250 KB
Volume
92
Category
Article
ISSN
0002-7863

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Oxidations by thionyl chloride. IV. Benz
โœ Arnold J. Krubsack; Tatsuo Higa ๐Ÿ“‚ Article ๐Ÿ“… 1972 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 160 KB

The reaction of hot thionyl chloride, in the presence of catalytic amounts of pyridine, on 3-phenylpropanoic acids constitutes one of the most direct routes to benso[&]thiophenes.2 It was of particular interest to us to extend this reaction to a variety of propanoic acids because the method showed p