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Oxidation of gem-Borylsilylalkylcoppers to Acylsilanes with Air.

✍ Scribed by Junichi Kondo; Hiroshi Shinokubo; Koichiro Oshima

Book ID
101996393
Publisher
John Wiley and Sons
Year
2006
Weight
29 KB
Volume
37
Category
Article
ISSN
0931-7597

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Backer1 reported in 1946 that potassium permanganate in acetone solution oxidized dimethylthiomethane (la) to the corresponding disulphoxide. -However, careful reinvestigation of this procedure in our laboratory demonstrated that the product was methylsulphonylmethylthiomethane (2a). -Although the