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Oxidation of Cedrane and Cedrol with iodine tris-(trifluoroacetate)

โœ Scribed by Acharan S. Narula; Elisabeth Trifilieff; Luu Bang; Guy Ourisson

Book ID
104235699
Publisher
Elsevier Science
Year
1977
Tongue
French
Weight
116 KB
Volume
18
Category
Article
ISSN
0040-4039

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Stereospecific Oxidation of Alkenes by I
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โœ Priv.-Doz. Dr. Joachim Buddrus ๐Ÿ“‚ Article ๐Ÿ“… 1973 ๐Ÿ› John Wiley and Sons ๐ŸŒ English โš– 197 KB

We have now prepared the ozonide (4), which appears to be an ideal starting material for the synthesis of (2). Compound ( 4 ) [m.p. 142ยฐC; NMR (CCl,): ~= 8 . 6 0 (6H), 8.73 (3H), 8.77 (3H), 9.07 (6H), 9.20 (6H)] is formed surprisingly smoothly by the action of AgBF, on the valence-isomeric ozonide (