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Oxidation of Aromatic and Aliphatic Triisopropylsilanylsulfanyls to Sulfonyl Chlorides: Preparation of Sulfonamides.

โœ Scribed by Yves Gareau; Jonathan Pellicelli; Sebastien Laliberte; Danny Gauvreau

Publisher
John Wiley and Sons
Year
2004
Weight
150 KB
Volume
35
Category
Article
ISSN
0931-7597

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The reduction of aliphatic and aromatic
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Amine N-oxides have been observed to be reduced by titanium(II1) chloride. To study this reaction, 24 model amine N-oxides were reacted with titanium(II1) chloride. The products of these reactions were shown by melting (boiling) points, mixed melting points, derivatives, refractive indices, infrared