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Oxidation and reduction of some derivatives of benzo-2,1,3-thiadiazole

โœ Scribed by I. A. Belen'kaya; N. S. Tsepova; Ya. L. Kostyukovskii; V. G. Pesin


Book ID
112326381
Publisher
Springer US
Year
1973
Tongue
English
Weight
349 KB
Volume
9
Category
Article
ISSN
0009-3122

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Disulfides of the benzo-2,1,3-thiadiazol
โœ I. A. Belen'kaya; T. A. Shulla ๐Ÿ“‚ Article ๐Ÿ“… 1989 ๐Ÿ› Springer US ๐ŸŒ English โš– 457 KB

A solution of 1 g (0.012 mole) of sodium nitrite in i0 ml of water was added to a hot solution of 2.7 g (0.01 mole) of 3-phenyl-4,5-dichloro-l,2,3-thiadiazolium chloride in 20 ml of 50% ethanol. The darkyellow precipitate was filtered, and recrystallized from a benzene-heptane (I:I) mixture. Yield,