ortho-Bis(dimethylsilyl)hexamethyldecasilasesquioxane
✍ Scribed by Bolte, Michael
- Book ID
- 104486587
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 319 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
Dichlorodimethylsilane is reacted with two equivalents of ketone enolates to give dimethylsilyl bis-enol ethers in good yields. Lithium tetramethylpiperidide (Li?Mp) as well as triethylamine (TEA) are used in deprotonation of ketones. An intramolecular aldol type of coupling has been achieved in an
Single-crystal X-ray study T = 100 K Mean (C-C) = 0.005 A R factor = 0.052 wR factor = 0.112 Data-to-parameter ratio = 10.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Di-l-fluoro-bis[(acetonitrile){N,N 0 0 0 -bis[(dimethylamino)(morpholino)methylene]propane-1,3-diamine}copper(II)] bis(hexafluorophosphate): the first di-l-fluoro-bridged dicopper bisguanidine compound