✦ LIBER ✦

Organic syntheses with isotopes. Part 1

✍ Scribed by Collins, Clair J.

Book ID: 125941955
Publisher: American Chemical Society
Year: 1959
Tongue: English
Weight: 993 KB
Volume: 36
Category: Article
ISSN: 0021-9584
DOI: 10.1021/ed036p205.1

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## Abstract A synthesis of oleic‐1‐^13^C acid and its conversion to triolein‐1′,1″,1″′‐^13^C~3~ are described. 9‐Octadecynenitrile‐1‐^13^C was prepared from 1‐bromo‐8‐heptadecyne and sodium cyanide‐^13^C. Hydrolysis afforded stearolic‐1‐^13^C acid, which was reduced to oleic‐1‐^13^C acid by the act