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Optimum levels of exchangeable protons in perdeuterated proteins for proton detection in MAS solid-state NMR spectroscopy

✍ Scribed by Ümit Akbey; Sascha Lange; W. Trent Franks; Rasmus Linser; Kristina Rehbein; Anne Diehl; Barth-Jan van Rossum; Bernd Reif; Hartmut Oschkinat


Publisher
Springer Netherlands
Year
2009
Tongue
English
Weight
407 KB
Volume
46
Category
Article
ISSN
0925-2738

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Dynamic parameters become more and more accessible in the study of uniformly isotopically enriched proteins by MAS solid-state NMR. We demonstrate that T 2 -related relaxation properties can quantitatively be determined in a sample of a perdeuterated microcrystalline protein by the measurement of 15