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Optimized Spectral Editing of 13C MAS NMR Spectra of Rigid Solids Using Cross-Polarization Methods

✍ Scribed by R. Sangill; N. Rastrupandersen; H. Bildsoe; H.J. Jakobsen; N.C. Nielsen


Publisher
Elsevier Science
Year
1994
Tongue
English
Weight
954 KB
Volume
107
Category
Article
ISSN
1064-1858

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A high-resolution 13C-nmr study of colla
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We have recorded high-resolution l3C-nmr spectra of collagen fibrils in the solid state by the cross-polarization-magic-angle-spinning (CP-MAS) method and analyzed the spectra with reference to those of collagenlike polypetides. We used two kinds of model polypeptides to obtain reference 13C chemica