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Optimization of the Oxidative Folding Reaction and Disulfide Structure Determination of Human α-Defensin 1, 2, 3 and 5

✍ Scribed by Shigeru Kubo; Kyoko Tanimura; Hideki Nishio; Naoyoshi Chino; Tadashi Teshima; Terutoshi Kimura; Yuji Nishiuchi


Book ID
106452204
Publisher
Springer Netherlands
Year
2008
Tongue
English
Weight
449 KB
Volume
14
Category
Article
ISSN
1573-3149

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✍ J. Vasu; Pradeep J. Nadkarni; Girish K. Trivedi; Alois Steigel 📂 Article 📅 1991 🏛 John Wiley and Sons 🌐 English ⚖ 368 KB

## Abstract (±)‐4,5,5‐Trimethyl‐1‐pyrroline‐1‐oxide reacted readily with ethyl 4,5,6,7‐tetra‐__O__‐acetyl‐__trans__‐2,3‐dehydro‐2,3‐dideoxy‐L(−)‐arabinoheptenoate in anhydrous benzene to give a mixture of two diastereomeric isoxazolidines, [2α,3β,3aα,5α]‐ and [2α,3β,3aα,5β]‐ethyl hexahydro‐2‐(1,2,3